NMR Laboratory
NMR Spectroscopy Laboratory of the Jagiellonian Center of Innovation has an Avance III HD 400 MHz (Bruker) spectrometer equipped with gradient probes working in a mode of normal (BBO) and reverse (BBI) detection. Both probes allow for measurement of H spectra and spectra of other nuclei (wide-spectrum probes).
The equipment enables:
- Identification of chemical substances with determination of chemical structure, often also of spatial structure and purity of compounds.
- Performing measurements in the temperature range from -150 to + 150ºC,
- measurement of 1D and 2D NMR spectra, including special correlation measurements:
- 1D: 1H, 13C, 19F, 1H{19F}, 19F{1H}, 31P, and more rarely: 11B, 29Si, 77Se, 119Sn, solvent suppression 1H, NOE, also DEPT at request
- 2D: COSY, DQCOSY, NOESY, ROESY, ss-TOCSY, ss-ROESY, [H-C]HMBC, [H-C]HMBC1j, [H-C]HSQC, [H-C]HSQCTOCSY, [H-N]HMBC, [H-N]HSQC, [H-F]HOESY
We offer:
- Determination and confirmation of chemical structure of organic compounds
- Determination of spatial structure and isomerism of organic compounds
- Confirmation of the chemical identity of samples
- Analysis of dynamic processes in chemical compounds
- Analysis of chemical preparation purity
Prices
- Standard analysis: 1H, 13C, F, P -> price: 33 PLN net per spectrum
- Analysis with guaranteed time – result within 12 hours from the moment when JCI obtained the sample* -> price: 60 PLN net per spectrum
Terms:
- Guaranteed time analysis of 13C, maximum 5 samples per day, each with a minimum of 20 mg of substance for analysis
- Guaranteed time analysis of 1H, maximum 20 samples per day, each with a minimum of 2 mg of substance for analysis
- URGENT analysis – result within 4 hours from the moment when JCI obtained the sample* -> price: 150 PLN net per spectrum
Terms:
- Guaranteed time analysis of 13C, maximum 1 sample per day, a minimum of 20 mg of substance for analysis
- Guaranteed time analysis of 1H, maximum 10 samples per day, each with a minimum of 2 mg of substance for analysis
- Before sending your samples for analysis, please contact the Head of the NMR Laboratory, Marek Żylewski, PhD
Note! For our regular clients, the results can be provided via FTP.
* If the sample is submitted to JCI on Friday after 12:00 noon, the result will be ready on Monday before 12:00.
The Head of the NMR Laboratory
Marek Żylewski, PhD
Holder of PhD in pharmaceutics with an extensive experience in NMR spectroscopy research. He obtained his PhD at the Faculty of Pharmacy of the Jagiellonian University Medical College, where he worked from 1997, and beginning from 2007 he was the head of NMR Spectroscopy Laboratory of the Faculty of Pharmacy of the Jagiellonian University Medical College. In his scientific work, he was involved in application of NMR spectroscopy in structural analysis of organic compounds. A co-author of more than 20 scientific papers. He has been working in the Jagiellonian Center of Innovation since 2013 as the head of the NMR Laboratory responsible for performing NMR analyses and solving structural problems.
For a quote, please contact:
Diana Dołęga, PhD
Mobile: +48 517 062 813
E-mail: diana.dolega@jci.pl
Our clients
Publications
Anna Jakubowska, Jorg Pabel, Marek Żylewski, Klaus T. Wanner, Katarzyna Kulig
Asymmetric synthesis of all four stereoisomers of 1-amino-3-hydroxy-cyclopentane-1-carboxylic acid
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